Investigation into the room temperature creep-deformation of potassium dihydrogen phosphate crystals using nanoindentation

doi:10.1007/s40436-018-0234-9

Advances in Manufacturing ›› 2018, Vol. 6 ›› Issue (4): 376-383.doi: 10.1007/s40436-018-0234-9

• ARTICLES • Previous Articles Next Articles

Investigation into the room temperature creep-deformation of potassium dihydrogen phosphate crystals using nanoindentation

Yong Zhang^1,2, Ning Hou^1,2,3, Liang-Chi Zhang³

1 School of Mechatronics Engineering, The Harbin Institute of Technology, Harbin 150001, People's Republic of China;
2 Ministry of Education Key Laboratory of Micro-systems and Micro-structures Manufacturing, The Harbin Institute of Technology, Harbin 150001, People's Republic of China;
3 Laboratory for Precision and Nano Processing Technologies, School of Mechanical and Manufacturing Engineering, The University of New South Wales, Sydney, NSW 2052, Australia

Received:2018-04-20 Revised:2018-09-28 Online:2018-12-25 Published:2018-12-08
Contact: Ning Hou,houning3393@163.com;Liang-Chi Zhang,liangchi.zhang@unsw.edu.au E-mail:houning3393@163.com;liangchi.zhang@unsw.edu.au
Supported by:
This work was funded as part of the DFG Project "Efficient determination of Stability Lobe Diagrams" (Grant No. BR 2905/73-1).

Abstract

Abstract: It has been a tremendous challenge to manufacture damage-free and smooth surfaces of potassium dihydrogen phosphate (KDP) crystals to meet the requirements of high-energy laser systems. The intrinsic issue is whether a KDP crystal can be plastically deformed so that the material can be removed in a ductile mode during the machining of KDP. This study investigates the room temperature creep-deformation of KDP crystals with the aid of nanoindentation. A stress analysis was carried out to identify the creep mechanism. The results showed that KDP crystals could be plastically deformed at the nanoscale. Dislocation motion is responsible for creep-deformation. Both creep rate and creep depth decrease with decrease in peak force and loading rate. Dislocation nucleation and propagation bring about pop-ins in the loaddisplacement curves during nanoindentation.

The full text can be downloaded at https://link.springer.com/article/10.1007/s40436-018-0234-9

Key words: Potassium dihydrogen phosphate (KDP) crystals, Creep-deformation, Stress, Dislocation

Yong Zhang, Ning Hou, Liang-Chi Zhang. Investigation into the room temperature creep-deformation of potassium dihydrogen phosphate crystals using nanoindentation[J]. Advances in Manufacturing, 2018, 6(4): 376-383.

TrendMD

References

1. de Yoreo J, Burnham AK, Whitman PK (2002) Developing KH₂PO₄ and KD₂PO₄ crystals for the world's most power laser. Int Mater Rev 47(3):113-152
2. Hawley-Fedder RA, Geraghty P, Locke SN et al (2004) NIF pockels cell and frequency conversion crystals. Int Soc Opt Photon. https://doi.org/10.1117/12.538482
3. Chen WQ, Lu LH, Liang YC et al (2015) Flatness improving method of KDP crystal in ICF system and its implementation in machine tool design. Proc Inst Mech Eng Part E J Process Mech Eng 229(4):327-332
4. Chen GD, Sun YZ, An CH et al (2016) Measurement and analysis for frequency domain error of ultra-precision spindle in a flycutting machine tool. Proc Inst Mech Eng Part B J Eng Manuf. https://doi.org/10.1177/0954405416673102
5. Chen GD, Sun YZ, Zhang FH et al (2017) Influence of ultraprecision flycutting spindle error on surface frequency domain error formation. Int J Adv Manuf Technol 88(9-12):3233-3241
6. Fang T, Lambropoulos JC (2002) Microhardness and indentation fracture of potassium dihydrogen phosphate (KDP). J Am Ceram Soc 85(1):174-178
7. Kucheyev SO, Siekhaus WJ, Land TA et al (2004) Mechanical response of KD_2xH_2(1-x)PO₄ crystals during nanoindentation. Appl Phys Lett 84(13):2274-2276
8. Guo XG, Zhang XJ, Tang XZ et al (2013) Nanoindentation on the doubler plane of KDP single crystal. J Semicond 34(3):034001
9. Lu C, Gao H, Wang J et al (2010) Mechanical properties of potassium dihydrogen phosphate single crystal by the nanoindentation technique. Mater Manuf Processes 25(8):740-748
10. Joshi MS, Antony AV, Rao PM (1980) Microhardness investigations on potassium dihydrogen phosphate crystals. Cryst Res Technol 15(6):743-746
11. Zhang Y, Zhang L, Liu M et al (2016) Revealing the mechanical properties of potassium dihydrogen phosphate crystals by nanoindentation. J Mater Res 31(8):1-9
12. Guin CH, Katrich MD, Savinkov AI et al (1980) Plastic strain and dislocation structure of the KDP group crystals. Cryst Res Technol 15(4):479-488
13. Peng J, Zhang LC, Lu XC (2013) Elastic-plastic deformation of KDP crystals under nanoindentation. Mater Sci Forum 773-774:705-711
14. Raman V, Berriche R (1992) An investigation of the creep processes in tin and aluminum using a depth-sensing indentation technique. J Mater Res 7(3):627-638
15. Mahmudi R, Roumina R, Raeisinia B (2004) Investigation of stress exponent in the power-law creep of Pb-Sb alloys. Mater Sci Eng A 382(1-2):15-22
16. Fu YJ, Gao ZS, Sun X et al (2000) Effects of anions on rapid growth and growth habit of KDP crystals. Prog Cryst Growth Charact Mater 40(1-4):211-220
17. Li H, Ngan AHW (2004) Size effects of nanoindentation creep. J Mater Res 19(02):513-522
18. Wang CL, Zhang M, Nieh TG (2009) Nanoindentation creep of nanocrystalline nickel at elevated temperatures. J Phys D Appl Phys 42(11):115405
19. Pešička J, Kužel R, Dronhofer A et al (2003) The evolution of dislocation density during heat treatment and creep of tempered martensite ferritic steels. Acta Mater 51(16):4847-4862
20. Pelleg J (2013) Mechanical properties of materials. Springer, Dordrecht
21. William D, Callister J, David G et al (2009) Materials science and engineering:an introduction. Wiley, New Jersey, pp 265-268
22. Lucas BN, Oliver WC (1999) Indentation power-law creep of high-purity indium. Metall Mater Trans A 30(3):601-610
23. Hosford WF (1967) Mechanical behavior of materials. Mater Today 20(5):83-85
24. Meyers MA, Chawla KK (2009) Mechanical behavior of materials. Cambridge University Press, Cambridge, pp 673-674
25. Hou N, Zhang Y, Zhang L et al (2016) Assessing microstructure changes in potassium dihydrogen phosphate crystals induced by mechanical stresses. Scripta Mater 113:48-50
26. Cao Z, Ju X, Yan C et al (2015) Synchrotron micro-XRF study of metal inclusions distribution in potassium dihydrogen phosphate (KDP) induced by ultraviolet laser pulses. Opt Mater Express 5(10):2201-2208
27. Johnson KL (1970) The correlation of indentation experiments. J Mech Phys Solids 18(2):115-126
28. Li WB, Henshall JL, Hooper RM et al (1991) The mechanisms of indentation creep. Acta Metal Mater 39(12):3099-3110
29. Frost HJ, Ashby MF (1982) Deformation mechanism maps:the plasticity and creep of metals and ceramics. Pergammon Press, Oxford
30. Alden TH (1987) Theory of mobile dislocation density:application to the deformation of 304 stainless steel. Metall Trans 18A:51-62
31. Wang SH, Chen W (2001) Room temperature creep deformation and its effect on yielding behaviour of a line pipe steel with discontinuous yielding. Mater Sci Eng A 301(2):147-153
32. Chang L, Zhang L (2009) Mechanical behaviour characterization of silicon and effect of loading rate on pop-in:a nanoindentation study under ultra-low loads. Mater Sci Eng A 506:125-129
33. Borc J, Sangwal K, Pritula I et al (2017) Investigation of pop-in events and indentation size effect on the (001) and (100) faces of KDP crystals by nanoindentation deformation. Mater Sci Eng A 708:1-10

[1]	Ping Zhou, Zi-Guang Wang, Ying Yan, Ning Huang, Ren-Ke Kang, Dong-Ming Guo. Sensitivity analysis of the surface integrity of monocrystalline silicon to grinding speed with same grain depth-of-cut [J]. Advances in Manufacturing, 2020, 8(1): 97-106.
[2]	Xiao-Liang Shi, Shi-Chao Xiu, Hui-Ling Su. Residual stress model of pre-stressed dry grinding considering coupling of thermal, stress, and phase transformation [J]. Advances in Manufacturing, 2019, 7(4): 401-410.
[3]	Yong Zhang, Ning Hou, Liang-Chi Zhang. Understanding the formation mechanism of subsurface damage in potassium dihydrogen phosphate crystals during ultraprecision fly cutting [J]. Advances in Manufacturing, 2019, 7(3): 270-277.
[4]	Heng Li, Tian-Jun Bian, Chao Lei, Gao-Wei Zheng, Yu-Fei Wang. Dynamic interplay between dislocations and precipitates in creep aging of an Al-Zn-Mg-Cu alloy [J]. Advances in Manufacturing, 2019, 7(1): 15-29.
[5]	Chuan Wu, Qing-Ling Meng. Microstructural evolution of a steam-turbine rotor subjected to a water-quenching process: numerical simulation and experimental verification [J]. Advances in Manufacturing, 2019, 7(1): 84-104.
[6]	V. G. Ladeesh, R. Manu. Effect of machining parameters on edge-chipping during drilling of glass using grinding-aided electrochemical discharge machining (G-ECDM) [J]. Advances in Manufacturing, 2018, 6(2): 215-224.
[7]	Li-Yao Gu, Min-Jie Wang. Adiabatic shear fracture prediction in high-speed cutting at various negative rake angles and feeds [J]. Advances in Manufacturing, 2018, 6(1): 41-51.
[8]	A. Pramanik, A. R. Dixit, S. Chattopadhyaya, M. S. Uddin, Yu Dong, A. K. Basak, G. Littlefair. Fatigue life of machined components [J]. Advances in Manufacturing, 2017, 5(1): 59-76.
[9]	Ying Fu, Wen-Ya Li, Xia-Wei Yang, Tie-Jun Ma, Achilles Vairis. The effects of forging pressure and temperature field on residual stresses in linear friction welded Ti6Al4V joints [J]. Advances in Manufacturing, 2016, 4(4): 314-321.
[10]	Jan C. Aurich, Marco Zimmermann, Stefan Schindler, Paul Steinmann. Turning of aluminum metal matrix composites: influence of the reinforcement and the cutting condition on the surface layer of the workpiece [J]. Advances in Manufacturing, 2016, 4(3): 225-236.
[11]	Nejah Tounsi, Tahany El-Wardany. Finite element analysis of chip formation and residual stresses induced by sequential cutting in side milling with microns to submicron uncut chip thickness and finite cutting edge radius [J]. Advances in Manufacturing, 2015, 3(4): 309-322.
[12]	Shou-Xu Song, Yun-Dong Liu,Qing-Di Ke,Ye-Chao Shen. Overlaying welding technology and performance of axle tube remanufacturing [J]. Advances in Manufacturing, 2013, 1(2): 143-150.

Investigation into the room temperature creep-deformation of potassium dihydrogen phosphate crystals using nanoindentation

PDF

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 12

Recommended Articles

Metrics

Comments